Study Programmes 2015-2016
WARNING : 2014-2015 version of the course specifications
Analytical chemistry: instrumental techniques
Duration :
44h Pr
Number of credits :
Master en bioingénieur : chimie et bioindustries, à finalité8
Lecturer :
Stéphanie Heuskin, Georges Lognay
Coordinator :
Language(s) of instruction :
French language
Units courses prerequisite and corequisite :
Prerequisite or corequisite units are presented within each program
Course contents :
LECTURES (Hybrid course): in French Electroanalytical chemistry : voltammetry, polarography, potentiometry and conductimetry.
Atomic emission spectrometry (flame). Atomic absorption spectrometry (principles, technical description and applications). Cases analysis, Food and agri-environmental applications. SEMINARS : Introduction to Near Infra-red spectrometry and Plasma atomic emission spectrometry. Practical works : LABORATORY EXERCISES in quantitative electrochemical analysis, Atomic emission and absorption spectrometry. LECTURES (Hybrid course): in English ( see also synopsis LANG2954-1) Introduction to ICP-MS ( 3h ) Group work ( 2 students): bibliographic research on the ICP-MS analysis of one element (analysis, application and comparison with other analytical techniques) Final presentation (3 pages) on the methodology.
Learning outcomes of the course :
To provide the student with an introduction to the principles of instrumental analysis (electrochemistry, molecular and atomic spectrometry) with special attention to their strengths and performances. After completing the course the student is expected to - demonstrate a good knowledge of the principles of quantitative electrochemical and spectrophotometric (molecular and atomic) methods of analysis; - develop a practical know-how in electrochemistry and spectrophotometry (molecular and atomic); - evaluate the experimental data; - understand the theorical and practical aspects of near infrared spectrometry and ICP-MS
Prerequisite knowledge and skills :
-- CHIM9242-4- Fundamentals of quantitative analytical chemistry
Planned learning activities and teaching methods :
Face-to-face and laboratory exercises
It is compulsary to attend all laboratory exercises
Mode of delivery (face-to-face ; distance-learning) :
Lectures : 20h
Practical Works : 44h
Seminars : 8h
Recommended or required readings :
1. Skoog, Holler et Nieman (2003). Principes d'analyse instrumentale; 1ère Edition; Editions De Boeck Université, ISBN 2-7445-0112-3 (recommended book) 2. J-P. Barthélemy (2006). Notes de TP de Chimie analytique quantitative à l'usage des 2ème Ing Chimie et Bio-industries. Electrochimie et méthode optique d'analyse. 3. Lecture notes 4. Copy of the didactical supports (available on e-campus, Blackboard plateform)
Assessment methods and criteria :
Oral examination (65%)
Personal report (35%)
Work placement(s) :
No training
Organizational remarks :
Contacts :
Lognay, Georges (Professeur Ordinaire)
+32 81/62.22.20