University of Liege | Version française
Academic year 2014-2015Value date : 1/10/2014
CHIM9246-2  Electrochemistry and atomic spectrometry

Duration :  20h Th, 44h Pr, 8h SEM
Number of credits :  
Master in Chemistry and Bio-industries, Professional Focus, 1st year5
Lecturer :  Georges Lognay
Language(s) of instruction :  
French language
Organisation and examination :  
Teaching in the first semester, review in January
Course contents :  
LECTURES (Hybrid course): in French Electroanalytical chemistry : voltammetry, polarography, potentiometry and conductimetry.
Atomic emission spectrometry (flame). Atomic absorption spectrometry (principles, technical description and applications). Cases analysis, Food and agri-environmental applications. SEMINARS : Introduction to Near Infra-red spectrometry and Plasma atomic emission spectrometry. Practical works : LABORATORY EXERCISES in quantitative electrochemical analysis, Atomic emission and absorption spectrometry. LECTURES (Hybrid course): in English ( see also synopsis LANG2954-1) Introduction to ICP-MS ( 3h ) Group work ( 2 students): bibliographic research on the ICP-MS analysis of one element (analysis, application and comparison with other analytical techniques) Final presentation (3 pages) on the methodology.
Learning outcomes of the course :  
To provide the student with an introduction to the principles of instrumental analysis (electrochemistry, molecular and atomic spectrometry) with special attention to their strengths and performances. After completing the course the student is expected to - demonstrate a good knowledge of the principles of quantitative electrochemical and spectrophotometric (molecular and atomic) methods of analysis; - develop a practical know-how in electrochemistry and spectrophotometry (molecular and atomic); - evaluate the experimental data; - understand the theorical and practical aspects of near infrared spectrometry and ICP-MS
Prerequisites and co-requisites/ Recommended optional programme components :  
-- CHIM9242-4- Fundamentals of quantitative analytical chemistry
Planned learning activities and teaching methods :  
Face-to-face and laboratory exercises
It is compulsary to attend all laboratory exercises
Mode of delivery (face-to-face ; distance-learning) :  
Lectures : 20h
Practical Works : 44h
Seminars : 8h
Recommended or required readings :  
1. Skoog, Holler et Nieman (2003). Principes d'analyse instrumentale; 1ère Edition; Editions De Boeck Université, ISBN 2-7445-0112-3 (recommended book) 2. J-P. Barthélemy (2006). Notes de TP de Chimie analytique quantitative à l'usage des 2ème Ing Chimie et Bio-industries. Electrochimie et méthode optique d'analyse. 3. Lecture notes 4. Copy of the didactical supports (available on e-campus, Blackboard plateform)
Assessment methods and criteria :  
Oral examination (65%)
Personal report (35%)
Work placement(s) :  
No training
Organizational remarks :  
Contacts :  
Lognay, Georges (Professeur Ordinaire)
+32 81/62.22.20
Georges.Lognay@ulg.ac.be



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